Multiscale Structural and Microstructural Investigation of Ternary Blends of Sawdust Ash and Sponge Gourd Ash in Concrete
DOI:
https://doi.org/10.33003/fjs-2026-1008-5341Keywords:
Pozzolanic Activity, Sawdust Ash (SDA), Sponge Gourd Ash (SGA), Sustainable Concrete, Ternary Blended ConcreteAbstract
Concrete production contributes significantly to global CO₂ emissions due to the energy-intensive manufacture of ordinary Portland cement (OPC), necessitating the development of sustainable cementitious alternatives. This study evaluates the performance of a novel agro-waste-based ternary supplementary cementitious material (SCM) system comprising sawdust ash (SDA) and sponge gourd ash (SGA) as partial replacements for OPC in concrete. A total OPC replacement level of 15% was adopted, with SGA contents ranging from 2.5% to 12.5% and SDA constituting the balance, along with a control mix containing 100% OPC. Fresh, mechanical, and microstructural properties were investigated up to 180 days of curing. The results revealed continuous strength development in all mixes, confirming sustained pozzolanic activity. At 180 days, the control concrete attained a compressive strength of 35.70 MPa, while the blended concretes achieved strengths ranging from 29.54 to 33.10 MPa. Among the ternary blends, the 2.5% SGA mix recorded the highest compressive strength of 32.40 MPa, representing only a 9.2% reduction relative to the control despite a 15% reduction in OPC content. Corresponding 180-day splitting tensile and flexural strengths ranged from 2.81–3.07 MPa and 3.01–3.56 MPa, respectively. Strong predictive relationships were established between compressive strength and splitting tensile strength (R² = 0.8739–0.9133), compressive strength and flexural strength (R² = 0.9792–0.9979), and splitting tensile strength and flexural strength (R² = 0.8874–0.9770). SEM analysis revealed progressive pore refinement and matrix densification as the curing age increased.
References
ACI Committee 318. Building Code Requirements for Structural Concrete and Commentary (ACI 318-19). American Concrete Institute, USA, 2019.
American Concrete Institute. ACI 213: Guide for structural lightweight aggregate concrete. ACI, 2003.
Akinyemi, B. A., & Dai, C. “Luffa cylindrical fibre as a natural reinforcement for cement composites: A review”. Journal of Sustainable Cement-Based Materials, vol. 11, no. 5, pp. 297–307, 2021. https://doi.org/10.1080/21650373.2021.1952658
Arıoğlu, N., Girgin, Z. C., & Arıoğlu, E. “Evaluation of ratio between splitting tensile strength and compressive strength for concretes up to 120 MPa and its application in strength criterion”. ACI Materials Journal, vol. 103, no. 1, pp. 18–24, 2006.
Assiamah, S., Agyeman, S., Adinkrah-Appiah, K., & Danso, H. “Utilization of sawdust ash as cement replacement for landcrete interlocking blocks production and mortarless construction”. Case Studies in Construction Materials, vol. 16, e00945, 2022. https://doi.org/10.1016/j.cscm.2022.e00945
Assiamah, S., Kankam, C. K., Adinkrah-Appiah, K., Afrifa, R. O., Banahehe, O. J., & Agyeman, S. “The impact of burnt sawdust ash from timber species as partial cement replacements on the durability properties for sustainable interlocking blocks”. Discover Civil Engineering, vol. 2, no. 20, 2025.
ASTM International. ASTM C33/C33M-18: Standard specification for concrete aggregates.
ASTM International (2018). https://doi.org/10.1520/C0033_C0033M-18
ASTM International. ASTM C136/C136M-19: Standard test method for sieve analysis of fine and coarse aggregates. ASTM International, 2019. https://doi.org/10.1520/C0136_C0136M-19
ASTM International. ASTM C1602/C1602M-12: Standard specification for mixing water used in the production of hydraulic cement concrete. ASTM International, 2012. https://doi.org/10.1520/C1602_C1602M-12
ASTM International. ASTM C618-05: Standard specification for coal fly ash and raw or calcined natural pozzolan for use in concrete. ASTM International, 2005.
ASTM International. ASTM C618-08: Standard specification for coal fly ash and raw or calcined natural pozzolan for use in concrete. ASTM International, 2008.
ASTM International. ASTM C618-19: Standard specification for coal fly ash and raw or calcined natural pozzolan for use in concrete. ASTM International, 2019. https://doi.org/10.1520/C0618-19
ASTM International. ASTM C618-22: Standard specification for coal fly ash and raw or calcined natural pozzolans for use in concrete. ASTM International, 2022.
Ayuba, A., Mohammed, B. S., & Liew, M. S. “Performance of blended cement systems incorporating agricultural waste ashes”. Construction and Building Materials, vol. 318, 125978, 2022.
Ayuba, S., & Ngabea, S. A. “The characteristic properties of self-compacting concrete (SCC) with sawdust ash (SDA) and millet husk ash (MHA) as cement replacement ternary blend”. FUW Trends in Science & Technology Journal, vol. 8, no. 2, pp. 196–202, 2023.
British Standards Institution. BS 12: Specification for Portland cement. BSI, 1996.
British Standards Institution. BS EN 12350-1: Testing fresh concrete – Part 1. BSI, 2000.
British Standards Institution. BS EN 12350-2: Testing fresh concrete – Part 2: Slump test. BSI, 2019.
British Standards Institution. BS EN 12350-6: Testing fresh concrete – Part 6: Density. BSI, 2019.
British Standards Institution. BS EN 12390-3: Testing hardened concrete – Compressive strength of test specimens. BSI, 2019.
British Standards Institution. BS EN 196-3: Methods of testing cement – Determination of setting times and soundness. BSI, 2016.
British Standards Institution. BS EN 197-1: Cement – Composition, specifications and conformity criteria for common cements. BSI, 2011
British Standards Institution. BS EN 12390-5: Testing hardened concrete – Flexural strength of test specimens. BSI, 2019.
British Standards Institution. BS EN 12390-6: Testing hardened concrete – Tensile splitting strength of test specimens. BSI, 2019.
Enobong F. Udoumoh, Patrick O. Emaikwu, Patience O. Agada, & Theresa Subeno. “A Bayesian Simulation Approach to Modeling the Relationship Between Narcotic Drug Use Prevalence and Unemployment Rate Using Aggregate Data.” FUDMA Journal of Sciences, vol. 8, no. 3 (Special Issue), 2024.
Ettu, L. O., Ajoku, C. C., & Nwachukwu, K. C. “Strength and setting characteristics of concrete containing agricultural waste ashes.” International Journal of Engineering Research and Technology, vol. 2, no. 4, pp. 1–10, 2013.
Ettu, L. O., Ezeh, J. C., Anya, U. C., Nwachukwu, K. C., & Njoku, K. O. “Strength of ternary blended cement concrete containing Afikpo rice husk ash and sawdust ash.” International Journal of Engineering Science Invention, vol. 2, no. 4, pp. 38–42, 2024.
Ettu, L. O., Ibearugbulem, O. M., Njoku, K. O., Anyaogu, O. L., & Agbo, S. I. “Strength of ternary blended cement sandcrete containing Afikpo rice husk ash and sawdust ash.” American Journal of Engineering Research (AJER), vol. 2, no. 4, pp. 133–137, 2024.
Fapohunda, C., Akinbile, B., & Oyelade, A. “A review of the properties, structural characteristics, and application potentials of concrete containing wood waste as partial replacement of one of its constituent materials.” YBL Journal of Built Environment, vol. 6, no. 1, pp. 63–85, 2018.
Fapohunda, C. A., Akinbile, B. M., & Shittu, A. K. “Structural properties of concrete containing sawdust ash as partial replacement of cement.” International Journal of Sustainable Built Environment, vol. 8, no. 2, pp. 476–485, 2019.
Fapohunda, C. A., & Daramola, D. D. “Experimental study of some structural properties of concrete with fine aggregates replaced partially by pulverized termite mound (PTM).” Journal of King Saud University – Engineering Sciences, vol. 32, pp. 484–490, 2020.
Fapohunda, C. A., Osanyinlokun, O. E., & Abioye, A. O. “A review of structures and performance of ternary blends of rice husk ash and some wastes in concrete.” Electronic Journal of Structural Engineering, vol. 23, no. 4, pp. 75–78, 2023.
Fapohunda, C. A., & Oyediji, S. D. “Structural performance evaluation of concrete reinforced with sponge gourd (Luffa aegyptiaca) fibre.” Nnamdi Azikiwe Journal of Civil Engineering, vol. 3, no. 2, pp. 132–144, 2025.
Gambhir, M. L. Concrete Technology: Theory and Practice. McGraw-Hill Education (India), 2013.
Imageonyechere, I. C. “Properties of Sawdust Concrete”. Journal of Building Material Science, vol. 4, no. 2, pp. 1–9, 2022. https://doi.org/10.30564/jbms.v4i2.4818
Ikponmwosa, E. E., Falade, F. A., Fashanu, T., Ehikhuemehin, S., & Adesina, A. “Experimental and numerical investigation of the effect of sawdust ash on the performance of concrete”. Journal of Building Pathology and Rehabilitation, vol. 5, no. 15, 2020. https://doi.org/10.1007/s41024-020-00081-3
James, O. “Effect of rice husk ash on concrete produced with sawdust ash”. Michael Okpara University of Agriculture Repository, 2025. Retrieved April 16, 2025, from https://repository.mouau.edu.ng
Majeed, A. A. “Effect of fine agricultural waste ashes on workability and strength of concrete.” Journal of Sustainable Construction Materials, vol. 6, no. 1, pp. 44–52, 2024.
Melo, E. C. R., Camillo, M. O., Marcelino, P. R. C., Silva, R. B. S., Firmino, T. C., Ferreira de Oliveira, B., Profeti, D., Pereira, A. C., Monteiro, S. N., & Oliveira, M. P. “Influence of silanization treatment of sponge gourd (Luffa cylindrica) fibers on the reinforcement of polyester composites: A brief report”. Polymers, vol. 14, 3311, 2022. https://doi.org/10.3390/polym14163311
Mhaiskar, Y., & Naik, D. D. “Studies on correlation between flexural strength and compressive strength of concrete”. The Indian Concrete Journal, pp. 1–6, 2012.
Mirzaei, A., Ghebrab, T., & Fedler, C. B. “Review and evaluation of agricultural biomass ashes as supplementary cementitious materials for sustainable concrete”. Processes, vol. 13, no. 11, 3571, 2025.
Nair, D. G., Fraaij, A., Klaassen, A. A. K., & Kentgens, A. P. M. “A structural investigation relating to the pozzolanic activity of rice husk ashes”. Cement and Concrete Research, vol. 38, pp. 861–869, 2008.
Neville, A. M. Properties of Concrete (5th ed.). Pearson Education, 2011.
Oboh, I. O., & Aluyor, E. O. “Luffa cylindrica—An emerging cash crop”. African Journal of Agricultural Research, vol. 4, no. 8, pp. 684–688, 2019.
Oboh, I. O., Aluyor, E. O., & Audu, T. O. “Application of Luffa cylindrica in natural form as biosorbent to removal of divalent metals from aqueous solutions: Kinetic and equilibrium study”. In Environmental Sustainability, pp. 195–212. InTech, 2011.
Ogbonna, A. C., & Abubakar, M. “Influence of sugarcane bagasse ash and sawdust ash on characteristics of concrete bridge substructures exposed to crude oil contaminated environment”. Acta Technica Corviniensis – Bulletin of Engineering, vol. 12, no. 4, pp. 2–6, 2019.
Olu, O. O. “Effect of sawdust ash and eggshell powder on the properties of cement blends”. American Journal of Construction and Building Materials, vol. 4, no. 2, pp. 88–99, 2020.
Olugbenga, O. “Performance of ternary blended cement with agro-waste ashes.” Nigerian Journal of Engineering, vol. 26, no. 1, pp. 35–42, 2019.
Quadri, M. O., & Alabi, A. O. “Assessment of sponge gourd (Luffa aegyptiaca) fiber as a polymer reinforcement in concrete”. Journal of Civil Engineering Materials and Application, vol. 4, no. 2, pp. 125–132, 2020.
Raghav, A., Sharma, R., & Mehta, P. “Soundness and durability of cement blended with supplementary materials.” Materials Today: Proceedings, vol. 46, pp. 7654–7660, 2021.
Ramzi, H., Ahmed, S., & Khalil, M. “Volume stability of blended cement systems with pozzolanic materials.” Case Studies in Construction Materials, vol. 18, e02012, 2023.
Seki, Y., Sever, K., Erden, S., Sarikanat, M., Neser, G., & Ozes, C. “Characterization of Luffa cylindrica fibers and the effect of water aging on the mechanical properties of its composite with polyester”. Journal of Applied Polymer Science, vol. 123, no. 4, pp. 2330–2337, 2012.
Shen, J., Xie, Y. M., Huang, X., Zhou, S., & Ruan, D. “Mechanical properties of luffa sponge”. Journal of the Mechanical Behavior of Biomedical Materials, vol. 15, pp. 141–152, 2012.
Siqueira, G., Bras, J., & Dufresne, A. “Luffa cylindrica as a lignocellulose source of fiber, microfibrillated cellulose and cellulose nanocrystals”. BioResources, vol. 5, no. 2, pp. 727–740, 2010.
Wang, Y., Liu, Z., & Chen, H. “Effect of mineral additives on the soundness and hydration behaviour of cement.” Journal of Materials in Civil Engineering, vol. 36, no. 2, 04023456, 2024.
Wasiu, S. P., Fapohunda, C. A., & Madueke, C. I. “Investigation into the properties and structure of ternary blends of sawdust ash and sponge gourd ash in mortar”. Nnamdi Azikiwe University Journal of Civil Engineering (NAUJCVE), vol. 3, no. 2, pp. 116–131, 2025.
Yılmazoğlu, M. U., Türkel, I., Benli, A., Bayraktar, O. Y., Bilgehan, M., & Kaplan, G. “Sustainable enhancement of alkali-activated foam concrete using vegetable waste ash and fly ash: Improving mechanical, thermal, and durability properties”. Journal of Building Engineering, vol. 110, 113091, 2025.
Zhao, J., Liu, J., Gao, X., Zhang, H., Zhang, H., & Gu, X. “Effect of environmental condition on volume deformation of blended cement mortars containing blast furnace slag and steel slag powder”. Journal of Building Engineering, vol. 85, 108692, 2024.
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