SYNTHESIS, CHARACTERIZATION AND ANTIBACTERIAL STUDIES ON IRON (II) COMPLEX OF SCHIFF BASE DERIVED FROM ORTHOPHENYLENEDIAMMINE AND 2-NITROBENZALDEHYDE
Keywords:
Ligand, Complexes, Orthophenylenediammine, 2-NitrobenzaldehydeAbstract
The synthesis and characterization of Schiff base derived from Orthophenylenediammine and 2-Nitrobenzaldehyde and its Iron (II) complex were undertaken. It was prepared by the condensation reaction of Orthophenylenediammine and 2-Nitrobenzaldehyde. Its Iron (II) metal complex was synthesized by coupling Iron (II) chloride with the formed ligand. These ligands and their complexes were characterized on the basis of their melting point and Decomposition temperature of the Schiff base and metal(II) complexes respectively, infrared spectral analysis, Solubility test, conductivity Test and magnetic susceptibility measurement. The ligand was found to be yellow in colour with a percentage yield of 50% and melting point of 265ºC, The Iron (II) complex was found to be Redish brown in colour with 55% percentage yield and 300ºC decomposition temperature, The ligand and the Iron (II) complex were found to be insoluble in water, n-hexane and Acetone and slightly soluble in methanol and ethanol and completely soluble in Dimethyl sulphoxide, The Iron (II) complex was found to be paramagnetic in nature, A band at 1525cm-1 of the ligand showed that the Aldehyde coordinated with the primary amine.
Published
How to Cite
Issue
Section
FUDMA Journal of Sciences
How to Cite
Most read articles by the same author(s)
- Sani Muhammad, Muhammad Suleiman Darma, Al-Amin Bashir, SYNTHESIS AND CHARACTERIZATION OF SALICYLALDEHYDE AND 2,4-DINITROPHENYL HYDRAZINE SCHIFF BASE WITH ITS COBALT (II) AND MANGANESE (II) COMPLEXES , FUDMA JOURNAL OF SCIENCES: Vol. 8 No. 4 (2024): FUDMA Journal of Sciences - Vol. 8 No. 4
- Sani Muhammad, Midi Habshah, Ibrahim Babura Babangida, ROBUST WHITE’S TEST FOR HETEROSCEDASTICITY DETECTION IN LINEAR REGRESSION , FUDMA JOURNAL OF SCIENCES: Vol. 3 No. 2 (2019): FUDMA Journal of Sciences - Vol. 3 No. 2
- Sani Muhammad, Suleiman Shamsuddeen, Ismail G. Baoku, ROBUST PARAMETER ESTIMATION FOR RANDOM EFFECT PANEL DATA MODEL IN THE PRESENCE OF HETEROSCEDASTICITY AND INFLUENTIAL OBSERVATIONS , FUDMA JOURNAL OF SCIENCES: Vol. 4 No. 4 (2020): FUDMA Journal of Sciences - Vol. 4 No. 4
- Sani Muhammad, Suleiman Shamshuddeen, Ismail Gboyega Baoku, ROBUST PARAMETER ESTIMATION FOR RANDOM EFFECT PANEL DATA MODEL IN THE PRESENCE OF HETEROSCEDASTICITY AND INFLUENTIAL OBSERVATIONS , FUDMA JOURNAL OF SCIENCES: Vol. 5 No. 3 (2021): FUDMA Journal of Sciences - Vol. 5 No. 3
- A. Bashir, M. I. Bello, S. J. Mahmoud, Ahmed Hauwa Zailani, ANTIMALARIAL ACTIVITY OF DECOCTION FROM CARICA PAPAYA, PSIDIUM GUAJAVA AND MANGIFERA INDICA LEAVES IN MICE INFECTED WITH PLASMODIUM BERGHEI (NK-65) , FUDMA JOURNAL OF SCIENCES: Vol. 8 No. 3 (2024): FUDMA Journal of Sciences - Vol. 8 No. 3 (Special Issue)