MECHANOCHEMICAL SYNTHESIS AND CHARACTERIZATION OF PYRAZOLE AND PYRAZOLATES COMPLEXES OF ZINC (II) IONS

  • T. Abubakar
  • M. A. Kurawa
  • S. Isyaku
Keywords: Mechanochemical, Pyrazole, Pyrazolium Chloride, Grinding, Mechanochemical Elimination

References

Adams C. J., Kurawa M. A. and Orpen A. G., (2010). Coordination chemistry in the solid state: synthesis and interconversion of pyrazolium salts, pyrazole complexes, and pyrazolate MOFs. J. Royal Society of Chemistry. Dalton Trans., 39:6974–6984.

Adams C. J., Kurawa M. A., Lusi M. and Orpen A. G.,(2008). Solid State synthesis of coordination compounds from basic metal salts. Cryst. Eng Comm., 10:1790–1795

Alan L. Balch, (2009). Solid state synthesis of coordination compounds from basic metal salt. J. Angew. Chem., Int. Ed., 48:2641–2644.

Angelici, R.J. (1971). “Synthesis and Techniques in Inorganic Chemistry”, W. B. Savders Company, Dalton Trans. 2nd Edition, pp 115-125.

Antesberger J., G. W. V. Cave, M. C. Ferrarelli, M. W. Heaven, C. L. Raston and J. L. Atwood, (2005). Solvent-free, direct synthesis of supramolecular nano-capsules. Chem. Commun., 892–894.

Bahl A. and Bahl B. S. (2007). Advanced Organic Chemistry, S. C and and Company Ltd, Ram Nagar, New Delhi, 20th edition, pp 490 – 497.

Balema V. P., J. W. Wiench, M. Pruski and V. K. Pecharsky,(2002). Mechanochemically induced solid state generation of phosphorus ylides and the solvent-free witting reaction. Chem. Commun. Cambridge, Pp 45-47.

Chen T., B. Liang and X. Xin, (1997). Studies on Solid-Solid Reactions between 4-Methylbenzenamine and Copper (II)Chloridedihydrate, Cobalt (II)Chloridehexahydrate and

Groeneveld W.L, Okkersen H., and Reedijk J., (1976). Pyrazolato and related anions, salt of 4-nitropyrazole. Rec. Trav. Chim., 92:947.

Halcrow M. A., (2009). Pyrazole and pyrazolides-flexible synthons in self. In Heterocyclic chemistry. J. Dalton Trans.,2059 – 2073.

Kumar N. Sharma and Pareek A. (2013), synthesis of new Schiff base complexes and their applications. International Journal of Applied Research and Studies II (2):307-315.

Kuroda R., Yoshida J., Nakamura A. and Nishikiori S.I., (2009). Annealing assisted mechanochemical synthesis of transition-metal coordination compounds and co-crystal formation. J. Cryst. Eng. Comm., 11:427 – 432.

Lancashire R.J., (2015), Coordination Chemistry. Kingston, Jamaica. Available on www.chem.uwimona.edu.jm/spectra/Mag Mon.html.

Maurya R. C. and Rajput S., (2004), Oxovanadium (IV) complexes of bioinorganic and medicinal relevance: synthesis, characterization and 3D molecular modeling and analysis of some oxovanadium (IV) complexes involving O, O-donor environment, J. Mol. Struct . 687(1): 35–44.

Raman N., Jeyamurugan R., Rajkapoor, B. and Mitu, L. (2010). Novel metal- based pharmacologically dynamic agents of transition metal (II) complexes: Designing, synthesis, structural elucidation, DNA binding and photo-induced DNA cleavage: activity, Spectro chim. Acta, Part A 75(1):88-97.

See1 F., and Sperber V., (1968). Interpretation of NMR chemical shifts and magnetic susceptibilities. J. Angew. Chem., 80:38.

Sindhu Y., Athira C.J., Sujamol M. S., Selwin R.J. and Mohanan K., (2013). Synthesis, characterization, DNA cleavage, and antimicrobial studies of some transition metal complexes with a novel Schiff base derived from 2-aminopyrimidine, Synth. React. Inorg. Met-Org. Nano-Met. Chem. 43(3):226-23

Published
2023-04-11
How to Cite
AbubakarT., KurawaM. A., & IsyakuS. (2023). MECHANOCHEMICAL SYNTHESIS AND CHARACTERIZATION OF PYRAZOLE AND PYRAZOLATES COMPLEXES OF ZINC (II) IONS. FUDMA JOURNAL OF SCIENCES, 3(4), 98 - 104. Retrieved from https://fjs.fudutsinma.edu.ng/index.php/fjs/article/view/1626