EFFECT OF LOW-TEMPERATURE CARBURIZATION TREATMENT ON THE HARDNESS BEHAVIOR OF Alsl316 AUSTENITIC STAINLESS STEEL

  • Kamilu Adeyemi Bello Ahmadu Bello University, Zaria-Nigeria.
  • Ibrahim I. Abubakar Ahmadu Bello University, Zaria
  • Lateef O. Bello Ahmadu Bello University, Zaria-Nigeria.
  • Rayyan M. Dodo Ahmadu Bello University, Zaria-Nigeria.
  • Zahradeen Musa Ahmadu Bello University, Zaria-Nigeria.
  • Muhammad Nura Bala Federal Polytechnic Damaturu, Yobe State
  • M. A. Hayatu
Keywords: Carburizer, Energizer, Hardness, Low-Temperature, Treatment

Abstract

There has been significant progress in the surface modification of stainless steel in order to enhance its surface hardness without major loss in other important properties. In this work, the possibility of enhancing the hardness property of austenitic stainless steel through a low-temperature pack carburization process was explored and investigated. Taguchi approach with L9 orthogonal array was used to optimize the hardness property of the carburized steel via the manipulation of the process parameters viz: carburizing temperature (350, 450, 550 oC), carburizing time (8,16, 24hrs) and carburizer/energizer ratio (90:10, 80:20,70:30). The surface hardness profiles of the carburized layer were investigated. Taguchi analysis result shows that optimal hardness of 407Hv was achieved. The optimization of the carburized surface properties revealed that the carburizing temperature of 550 oC, carburizing time of 24hrs and carburizer/energizer ratio of 90:10 are the prominent factors and levels for achieving optimal condition respectively.  The models for optimal conditions were validated and the prediction adequacy are found to be within the limit of 2-6% prediction error, indicating the models are accurate and adequate to predict the responses. Optical microscope micrographs and morphologies indicates that the modified steel layer obtained at the optimal condition shows mild deeper case profile compared to non-treated stainless-steel samples. Equivalent of 104% improvement in the case hardness was achieved for the samples investigated with optimized condition. The level of improvement attained in the hardness therefore suggest that the ultimate objective of surface modification of austenitic stainless steel investigated in this study has been achieved.

Author Biographies

Kamilu Adeyemi Bello, Ahmadu Bello University, Zaria-Nigeria.

Professor with Metallurgical and Materials Engineering

Rayyan M. Dodo, Ahmadu Bello University, Zaria-Nigeria.

Reader with the Department of Metallurgical and Materials Engineering

Zahradeen Musa, Ahmadu Bello University, Zaria-Nigeria.

L I with Department of Metallurgical and Materials Engineering

Muhammad Nura Bala, Federal Polytechnic Damaturu, Yobe State

Assitant Lecturer with Department of Mechanical Engineering

References

Aydin, M., et al. (2015). Low-Temperature Carburizing of Stainless Steel. Journal of Materials Processing Technology, 228, 194-203. https://doi.org/10.1016/j.jmatprotec.2015.09.021 DOI: https://doi.org/10.1016/j.jmatprotec.2015.09.021

Baali, S., Benarioua, Y. and Mazouz, A.E. 2023. An Experimental Study of the Influence of Carburizing Treatment Holding Time on the Structure and Hardness of 16NC6 Steel. Engineering, Technology & Applied Science Research. 13, 2 (Apr. 2023), 1047810482. https://doi.org/10.48084/etasr.5684. DOI: https://doi.org/10.48084/etasr.5684

Chen, J., Zhu, Y., Chen, X., Ma, X., & Chen, B. (2023). Interfacial microstructure and cladding corrosion resistance of stainless steel/carbon steel clad plates at different rolling reduction ratios. Metals, 15(1), 16. https://doi.org/10.3390/met15010016 DOI: https://doi.org/10.3390/met15010016

Cheng, J., et al. (2018). Optimization of Carburizing Process Using Taguchi Method. Materials Science and Engineering, 701(1), 56-64. https://doi.org/10.1016/j.msea.2017.06.019 DOI: https://doi.org/10.1016/j.msea.2017.06.019

Dabbashi., S. (2023). Impact Of Carburizing Parameters on The Mechanical Properties of Carbon Steel Alloy (AISI 1025). International journal of creative research thoughts. 11, 10 (Oct. 2023), ISSN: 2320-2882.

Dahmardeh, M., et al. (2020). Chemical Composition and Characterization of AISI 316 Stainless Steel. Materials Testing, 62(6), 460-467. https://doi.org/10.3139/120.111494 DOI: https://doi.org/10.3139/120.111494

De la Rosa, Y. E. N., Calabokis, O. P., Borges, P. C., & Ballesteros, V. B. (2020). Effect of Low-Temperature Plasma Nitriding on Corrosion and Surface Properties of Duplex Stainless Steel UNS S32205. Journal of Materials Engineering and Performance, 29(4), 2612-2622. https://doi.org/10.1007/s11665-020-04753-6 DOI: https://doi.org/10.1007/s11665-020-04753-6

Goglia, M., et al. (2019). Carburization of Stainless Steel: Influence of Carburizer Composition. Materials Science and Engineering, 739, 85-93. https://doi.org/10.1016/j.msea.2018.10.098 DOI: https://doi.org/10.1016/j.msea.2018.10.098

Kim, S., et al. (2016). Effect of Surface Activation on Carburizing of Stainless Steels. Journal of Materials Engineering and Performance, 25(11), 5087-5095. https://doi.org/10.1007/s11665-016-2345-7

Lee, S., et al. (2015). Depth Profile Analysis of Carburized Stainless Steel. Metallurgical and Materials Transactions A, 46(5), 2223-2231. https://doi.org/10.1007/s11661-015-2847-9

Liu, X., et al. (2019). Surface Cleaning Methods in Metallurgical Treatments. Journal of Surface Engineering, 35(2), 123-130. https://doi.org/10.1080/02670844.2018.1479876

Liu, Zhe; Peng, Yawei; Chen, Chaoming; Gong, Jianming; Jiang, Yong (2020). Effect of surface nanocrystallization on low-temperature gas carburization for AISI 316L austenitic stainless steel. International Journal of Pressure Vessels and Piping, (), 104053. https://doi.org/10.1016/j.ijpvp.2020.104053 DOI: https://doi.org/10.1016/j.ijpvp.2020.104053

Lopez, H., Xie, C., Wu, S., Yu, Y., & Wang, G. (2023). Effect of in-situ rolling and heat treatment on microstructure, mechanical and corrosion properties of wire-arc additively manufactured 316L stainless steel. Journal of Materials Research and Technology, 27, 33493361. https://doi.org/10.1016/j.jmrt.2023.02.001 DOI: https://doi.org/10.1016/j.jmrt.2023.10.168

Luo, M., et al. (2020). Microstructure Evolution of Carburized Stainless Steel. Journal of Alloys and Compounds, 812, 151379. https://doi.org/10.1016/j.jallcom.2019.151379

Nouri, H., et al. (2016). Optimization of Hardness in Carburizing Stainless Steel Using Taguchi Method. International Journal of Advanced Manufacturing Technology, 85(1), 321-331. https://doi.org/10.1007/s00170-015-7956-3

Peng, X., et al. (2018). Machining of Stainless Steel: Influence of Process Parameters. Journal of Materials Processing Technology, 253, 72-81. https://doi.org/10.1016/j.jmatprotec.2017.10.015 DOI: https://doi.org/10.1016/j.jmatprotec.2017.10.015

Phadke, M. (1989). Quality Engineering Using the Taguchi Method. Prentice Hall.

Ramadan., N. (2023). Investigation of the Effect Of Temperature and Time of Case Hardening on the Mechanical Properties and Microstructure of Low Carbon Steel (AISI 1020). Surman Journal for Science and Technology.

Shin, D., et al. (2015). Effect of Barium Carbonate on Carburizing of Steel. Journal of Materials Science, 50(5), 2322-2332. https://doi.org/10.1007/s10853-014-8756-9

Srinivasan. N (2021). Sensitization of Austenitic Stainless Steels: Current Developments, Trends, and Future Directions. Metallography, Microstructure, and Analysis. 10(2), 133-147. https://doi.org/10.1007/s13632-021-00724-y DOI: https://doi.org/10.1007/s13632-021-00724-y

Tohidi, M., et al. (2017). Taguchi's Approach for Process Optimization in Heat Treatment of Steel. Journal of Manufacturing Processes, 30, 253-265. https://doi.org/10.1016/j.jmapro.2017.09.012 DOI: https://doi.org/10.1016/j.jmapro.2017.09.012

Xu, Y., et al. (2018). Surface Treatment of Austenitic Stainless Steel by Acid Pickling. Journal of Materials Science, 53(2), 1236-1245. https://doi.org/10.1007/s10853-017-1654-9 DOI: https://doi.org/10.1007/s10853-017-1654-9

Zhang, C., Jin, W., Jin, S., Tian, Y., Wellmann, D., & Liu, W. (2022). Wire arc additive manufacturing of stainless steels: a review. International Journal of Advanced Manufacturing Technology, 113, 24132431. https://doi.org/10.1007/s00170-021-06768-1

Zhou, L., et al. (2017). The Influence of Surface Activation on Carburizing Process of Austenitic Stainless Steel. Materials Science and Engineering A, 684, 209-215. https://doi.org/10.1016/j.msea.2016.12.099 DOI: https://doi.org/10.1016/j.msea.2016.12.099

Published
2025-03-31
How to Cite
Bello, K. A., Abubakar, I. I., Bello, L. O., Dodo, R. M., Musa, Z., Bala, M. N., & Hayatu, M. A. (2025). EFFECT OF LOW-TEMPERATURE CARBURIZATION TREATMENT ON THE HARDNESS BEHAVIOR OF Alsl316 AUSTENITIC STAINLESS STEEL. FUDMA JOURNAL OF SCIENCES, 9(3), 240 - 246. https://doi.org/10.33003/fjs-2025-0903-3244

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